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Article
Publication date: 7 February 2024

Nancy Sobh, Nagla Elshemy, Sahar Nassar and Mona Ali

Due to herbs and plants’ therapeutic properties and simplicity of availability in nature, humans have used them to treat a variety of maladies and diseases since ancient times…

Abstract

Purpose

Due to herbs and plants’ therapeutic properties and simplicity of availability in nature, humans have used them to treat a variety of maladies and diseases since ancient times. Later, as technology advanced, these plants and herbs gained significant relevance in some industries due to their suitable chemical composition, abundant availability and ease of access. Aegle marmelos is a species of plant that may be found in nature. Yet, little or very little literature was located on the coloration behavior of this plant’s leaves. This study aims to focus on the effect of different parameters on the extraction of colorant from Aegle marmelos leaves.

Design/methodology/approach

Some factors that affected on the extraction processes were examined and found to have significant impacts on the textile dyeing such as the initial dye concentration, extracted temperature, extracted bath pH and extracted time were all changed to see how they affected color extraction. The authors report a direct comparison between three heating methods, namely, microwave irradiation (MWI), ultrasonic waves (USW) and conventional heating (CH). The two kinetic models have been designed (pseudo-first and pseudo-second orders) in the context of these experiments to investigate the mechanism of the dyeing processes for fabrics under study. Also, the experimental data were analyzed according to the Langmuir and Freundlich isotherms.

Findings

From the result, it was discovered these characteristics were found to have a substantial effect on extraction efficiency. Temperature 90°C and 80°C when using CH and USW, respectively, while at 90% watt when using MWI, period 120 min when using CH as well as USW waves, while 40 min when using MWI, and pH 4, 5 and 10 for polyamide, wool and cotton, respectively, were the optimal extraction conditions. Also, the authors can say that wool gives a higher absorption than the other fabric. Additionally, MWI provided the best color strength (K/S) value, and homogeneity, at low temperatures reducing the energy and time consumed. The coloring follows the order: MWI > USW > CH. The adsorption isotherm of wool could be well fitted by Freundlich isotherm when applying CH and USW as a heating source, while it is well fitted by the Langmuir equation in the case of MWI. In the study, it was observed that the pseudo-first-order kinetic model fits better the experimental results of CH with a constant rate K1 = −0.000171417 mg/g.min, while the pseudo-second-order kinetic model fits better the experimental results of absorption of both MWI (K2 = 38.14022572 mg/g.min) and USW (K2 = 12.45343554 mg/g.min).

Research limitations/implications

There is no research limitation for this work. Dye was extracted from Aegle marmelos leaves by applying three different heating sources (MWI, ultrasonic waves [USWW] and CH).

Practical implications

This work has practical applications for the textile industry. It is concluded that using Aegle marmelose leaves can be a possible alternative to extract dye from natural resource by applying new technology to save energy and time and can make the process greener.

Social implications

Socially, it has a good impact on the ecosystem and global community because the extracted dye does not contain any carcinogenic materials.

Originality/value

The work is original and contains value-added products for the textile industry and other confederate fields.

Details

Pigment & Resin Technology, vol. ahead-of-print no. ahead-of-print
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 25 January 2011

Mun Teng Soo, Kuan Yew Cheon and Ahmad Fauzi Mohd Noor

The purpose of this paper is to report on metal‐oxide‐semiconductor (MOS) capacitor‐based O2 sensors with different catalytic metal electrode (Al or Pd), deposited on both smooth…

Abstract

Purpose

The purpose of this paper is to report on metal‐oxide‐semiconductor (MOS) capacitor‐based O2 sensors with different catalytic metal electrode (Al or Pd), deposited on both smooth and porous surface (pore diameter ranging from 2.76 to 71.6 μm) of ZrO2 thin film.

Design/methodology/approach

The ZrO2 thin film has been prepared by RF sputtering and DC magnetron sputtering process followed by thermal oxidation process, whereas the electrodes were deposited on thin film by thermal evaporation. The sensors are exposed to O2 gas ambient at room temperature and the O2 sensing performance has been examined by surface characterizations and on‐line sensing electrical characterizations.

Findings

MOS capacitor O2 sensor with Pd electrode on porous ZrO2 thin film has the best sensitivity in term of both adsorption and desorption of gas. This sensor is proved to be operated in both capacitor and diode modes.

Originality/value

The paper demonstrates that room temperature MOS‐based O2 sensor operates in capacitor and diode mode conditions with focus on the effect of ZrO2 surface morphology on the sensing properties.

Details

Microelectronics International, vol. 28 no. 1
Type: Research Article
ISSN: 1356-5362

Keywords

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